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Equine porphyrins. Co-oxidation of meso-tetraphenylporphyrin TPPH to form four different isomeric porphyrins has been undertaken. Small-molecular mass porphyrins in which a carboxylic acid group replaces the chlorine atom in TPPH have been prepared. The molecular masses of these compounds were determined by mass spectroscopy, and their structure was confirmed by single-crystal X-ray diffraction.
The porphyrins have been used to determine the excitation spectra of TPPH and its isomeric porphyrins. Spectral measurements were performed by flash photolysis, steady-state absorption, and steady-state fluorescence.
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